By David Mautner Himmelblau; James B Riggs
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Additional resources for Solutions manual to accompany Basic principles and calculations in chemical engineering, seventh edition
1-23). The result of this is that the two components of a quadrupole doublet may not be equal in intensity, thus increasing the difficulty in subsequent computational procedures. g. the presence of an additional component centered around the more intense peak might be assumed or a Goldanskii-Karyagin effect (19) (anisotropy of the recoil-free fraction) might be postulated. Various groups of workers have different methods for B. A. GOODMAN 26 ,--------I I I I VELOCITY TRANSDUCER LASER I I L ________ _ Figure 1-20.
T % refers to the percentage of the total Fe. x half widths constrained to be equal. The errors quoted in brackets include standard deviations and covariance contributions. 23 Chem. Fe 3+ Partly oxidized biotite (bedrock) Fresh biotite Sample Fe 3+ Table 1-5 continued. 68 (10) 49 (11 ) 33 (6) 26 (5) %I: 241 237 185 245 253 2 X v. =" 0 MOSSBAUER SPECTROSCOPY 51 Analytical results show that the other stages in the weathering sequence are also characterized by further oxidation and loss of iron (Table 1-5).
In designing an experimental set-up the separation of the source from the detector has to be carefully selected. Thus, although it is desirable to have them close together in order to maximize the count rate, placing them too close leads to broadening of the spectra. This is because the emitted 'Y-ray makes an angle fJ with the direction of motion of the source (Fig. 1-21), so that the energy shift due to the Doppler motion is (v/c)E'YcosfJ, where v, c, and E'Y have the same meanings as 23 MtlSSBAUER SPECTROSCOPY liquid nitrogen inlet sorb heat exchanger sample holder Figure 1-17.